THE FLUID INCLUSION PALEO PRESSURE CHARACTERISTICS AND GEOLOGICAL IMPLICATIONS OF GAOTAIZI TIGHT RESERVOIR IN QIJIA AREA OF SONGLIAO BASIN
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摘要: 流体包裹体热动力学(PVTx)模拟应用包裹体组分、均一温度和气液比,结合模拟软件可以恢复包裹体被捕获时的古流体压力,以松辽盆地齐家地区高台子致密油层为例,应用激光共聚焦扫描显微镜、显微荧光和显微测温等分析,划分了油气充注幕次并恢复了各幕次流体古压力,该应用有效区分了不同幕次流体古压力特征。研究结果表明:齐家地区高台子油层存在两期油气充注,第1期发生在晚白垩世嫩江晚期(79~75 Ma),主要充注发黄色荧光的原油,古流体压力为16.13~16.97 MPa;第2期发生在晚白垩世明水期(69~65 Ma),主要充注发黄绿色、蓝绿色荧光颜色的原油,古流体压力为22.14~26.13 MPa。研究结果有助于深化勘探区油气成藏规律的认识。Abstract: PVTx thermal dynamics simulation of reservoir fluid inclusions has been applied to restore trapping pressures by inclusion component, homogenization temperature and gas liquid ratio combined with simulation software. In Gaotaizi tight reservoir in Qijia area of Songliao Basin, the hydrocarbon charging events and the paleo fluid pressure are divided by CLSM, fluorescence microscopy and micro-thermometry, through which characteristics of different events of paleo fluid pressure are distinguished. The results indicate two stages of hydrocarbon charging in Qijia Area. The first charging occurred in upper Cretaceous Nenjiang late stage(79~75 Ma), with yellow fluorescence color. The second charging occurred in upper Cretaceous Mingshui stage(79~75 Ma), with yellow-green and blue-green fluorescence color. The paleo fluid pressures of two stages respectively are 16.13~16.97 MPa and 22.14~26.13 MPa.All the research findings are of great help to deepen the understanding of hydrocarbon accumulation patterns of the exploration area.
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Key words:
- fluid inclusion /
- PVTx simulation /
- paleo pressure /
- Qijia area /
- Gaotaizi reservoir
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图 4 PVTx热动力学模拟原理图(据参考文献[16]修改)
Figure 4.
表 1 齐家地区高台子油层油包裹体荧光参数
Table 1. The fluorescence parameters of oil inclusions in Gaotaizi reservoir in Qijia Area
烃类包裹体 荧光颜色 λmax/nm Q QF535 油包裹体 黄色 580.9~585.4 1.17~1.40 2.45~2.92 油包裹体 黄绿 520.6~545.4 0.37~0.77 1.25~1.77 油包裹体 蓝绿 489.3~519.7 0.12~0.50 0.50~1.24 表 2 共聚焦扫描显微镜精确测定的部分油包裹体气液比
Table 2. The gas-liquid ratios of part of the fluid inclusions by CLSM
井号 深度/m 层位 岩性 总体积/um3 气泡体/um3 气液比/% 齐平1 1952.69 高台子 粉砂岩 552.71 19.72 3.7 齐平1 1952.69 高台子 粉砂岩 651.25 47.12 7.8 齐平1 2071 高台子 粉砂岩 698.14 41.38 6.3 齐平1 2071 高台子 粉砂岩 889.56 40.74 4.8 金23 2205.3 高台子 细砂岩 519.56 27.55 5.6 金23 2205.3 高台子 细砂岩 700.74 39.67 6 英X53 2078 高台子 粉砂岩 1058.44 61.79 6.2 英X53 2078 高台子 粉砂岩 587.39 35.85 6.5 古94 2193.6 高台子 粉砂岩 696.48 40.04 6.1 古94 2193.6 高台子 粉砂岩 540.15 37.22 7.4 古94 2198.5 高台子 粉砂岩 575.14 39.13 7.4 金191 1839.7 高台子 细砂岩 758.13 40.20 5.6 金191 1854.5 高台子 粉砂岩 368.86 18.90 5.4 金34 2125 高台子 粉砂岩 324.02 22.61 7.5 金34 2135 高台子 粉砂岩 532.01 37.12 7.5 龙201 1935.07 高台子 粉砂岩 404.88 21.83 5.7 金28 2217.4 高台子 粉砂岩 528.13 28.48 5.7 表 3 模拟过程中原油样品成分组成表
Table 3. The Composition of crude oil sample in simulation
组分 摩尔组成百分比/% 组分 摩尔组成百分比/% CO2 0.84 n-C5 3.920 N2 0 C6 1.760 C1 26.570 C7 4.257 C2 10.740 C8 3.790 C3 9.270 C9 3.375 i-C4 0.520 C10 5.680 n-C4 6.300 C11+ 21.718 i-C5 1.260 — — 表 4 齐家地区高台子油层部分流体包裹体组合PVTx模拟参数和结果
Table 4. The PVTx simulation parameters and results of part fluid inclusion assemblages in Gaotaizi reservoir in Qijia Area
井号 层位 深度/m 第1幕 第2幕 第3幕 G/L/% Tho/Tha P/MPa Pc G/L/% Tho/Tha P/MPa Pc G/L/% Tho/Tha P/MPa Pc 齐平1 高台子 1952.69 3.7 68.2/86.3 16.97 1.29 7.8 89.5/101.0 23.86 1.28 齐平1 高台子 2071 6.3 85.9/107.1 24.75 1.37 4.8 95.7/133.4 24.02 1.33 金28 高台子 2205.3 5.6 80.6/106.2 25.54 1.34 6 105.3/137.3 24.93 1.35 英x58 高台子 2078 6.2 86.2/107.4 24.38 1.28 6.5 104.3/131.4 24.89 1.31 古94 高台子 2193.6 6.1 84.5/107.8 25.35 1.27 7.4 107.8/129.2 24.91 1.03 金191 高台子 1839.7 5.6 85.8/107.5 22.59 1.28 金34 高台子 2125 7.5 88.1/102.4 24.59 1.37 龙201 高台子 1935.07 3.2 62.7/81.5 16.13 1.21 金191 高台子 1854.5 5.2 82.1/106.1 22.94 1.31 古94 高台子 2198.50 7.4 104.0/127.9 25.98 1.26 金34 高台子 2135.0 7.5 79.3/107.0 24.96 1.30 金28 高台子 2217.40 5.7 102.0/137.9 26.13 1.25 注:G/L—气液比; Tho/Tha—油包裹体/同期盐水包裹体均一温度; Pc—古压力系数计算值; P—热动力学模拟获得的古压力 -
高瑞祺, 蔡希源.松辽盆地油气田形成条件与分布规律[M].北京:石油工业出版社, 1997.
GAO Ruiqi, CAI Xiyuan. The reservoir distribution rules and formation condition of Songliao Basin[M]. Beijing:Petroleum Industry Press, 1997. (in Chinese)
杨万里, 高瑞祺, 郭庆福, 等.松辽盆地陆相油气生成、运移和聚集[M].哈尔滨:黑龙江科学技术出版社, 1985.
YANG Wanli, GAO Ruiqi, GUO Qingfu, et al. The continental oil generation, migration and acumulation in Songliao Basin[M]. Harbin:Heilongjiang Science and Technology Press, 1985. (in Chinese)
Roedder E. Application of an improved crushing microscope stage to studies of gases in fluid inclusion[J]. SchweizerMineralog Petrog Mitt, 1970, 50:41~58. https://link.springer.com/chapter/10.1007/978-1-4612-3492-0_7
Coveney R M, Goebel E D, Ragan V M. Pressures and temperatures from aqueous fluid inclusions in sphalerite from Midcontinent country rocks[J]. Economic Geology, 1987, 82(3):740~751. doi: 10.2113/gsecongeo.82.3.740
Aplin A C, Macleod G, Larter S R, et al. Combined use of Confocal Laser Scanning Microscopyand PVT simulation for estimating the composition andphysical properties of petroleum in fluid inclusions[J]. Marine and Petroleum Geology, 1999, 16(2):97~110. doi: 10.1016/S0264-8172(98)00079-8
施立志, 王卓卓, 张革, 等.松辽盆地齐家地区致密油形成条件与分布规律[J].石油勘探与开发, 2015, 42(1):44~50. doi: 10.11698/PED.2015.01.05
SHI Lizhi, WANG Zhuozhuo, ZHANG Ge, et al. Distribution and formation of tight oil in Qijia area, Songliao Basin, NE China[J]. Petroleum Exploration and Development, 2015, 42(1):44~50. (in Chinese with English abstract) doi: 10.11698/PED.2015.01.05
陈方文, 卢双舫, 黄振凯, 等.松辽盆地古龙凹陷青一段沉积特征及有利勘探区[J].中南大学学报(自然科学版), 2013, 44(5):1955~1963. https://www.wenkuxiazai.com/doc/bfe7a9db804d2b160a4ec051.html
CHEN Fangwen, LU Shuangfang, HUANG Zhenkai, et al. Sedimentary characteristics and favorable exploration zone of K1qn1 in Gulong Depression of Songliao Basin[J]. Journal of Central South University (Science and Technology), 2013, 44(5):1955~1963. (in Chinese with English abstract) https://www.wenkuxiazai.com/doc/bfe7a9db804d2b160a4ec051.html
袁青, 罗群, 李楠, 等.齐家南地区高台子油层致密油成藏模式[J].特种油气藏, 2016, 23(1):54~57. http://d.old.wanfangdata.com.cn/Periodical/tzyqc201601012
YUAN Qing, LUO Qun, LI Nan, et al. Gaotaizi tight oil accumulation modes in southern Qijia[J]. Special Oil and Gas Reservoirs, 2016, 23(1):54~57. (in Chinese with English abstract) http://d.old.wanfangdata.com.cn/Periodical/tzyqc201601012
付秀丽.松辽盆地北部齐家地区高台子油层沉积体系展布及其成藏分析[J].成都理工大学学报(自然科学版), 2014, 41(4):422~427. http://d.old.wanfangdata.com.cn/Periodical/cdlgxyxb201404003
FU Xiuli. Distribution of Gaotaizi oil layers and accumulation analysis in qijia area of northern Songliao basin, China[J]. Journal of Chengdu University of Technology (Science & Technology Edition), 2014, 41(4):422~427. (in Chinese with English abstract) http://d.old.wanfangdata.com.cn/Periodical/cdlgxyxb201404003
王成, 宋桂霞, 刘振文.松辽盆地北部自生矿物包裹体研究及应用[J].大庆石油地质与开发, 1994, 13(4):19~22. http://kns.cnki.net/KCMS/detail/detail.aspx?filename=dqsk404.005&dbname=CJFD&dbcode=CJFQ
WANG Cheng, SONG Guixia, LIU Zhenwen. Enclosure of authigenic mineral from northern part of Songliao basin and its application[J]. Petroleum Geology and Oilfield Development in Daqing, 1994, 13(4):19~22. (in Chinese with English abstract) http://kns.cnki.net/KCMS/detail/detail.aspx?filename=dqsk404.005&dbname=CJFD&dbcode=CJFQ
蒙启安, 白雪峰, 梁江平, 等.松辽盆地北部扶余油层致密油特征及勘探对策[J].大庆石油地质与开发, 2014, 33(5):23~29. http://d.old.wanfangdata.com.cn/Periodical/dqsydzykf201405005
MENG Qi'an, BAI Xuefeng, LIANG Jiangping, et al. Fuyu tight oil characteristics and exploration countermeasures in north songliao basin[J]. Petroleum Geology and Oilfield Development in Daqing, 2014, 33(5):23~29. (in Chinese with English abstract) http://d.old.wanfangdata.com.cn/Periodical/dqsydzykf201405005
王雅春, 王胜男.源岩、超压和断裂空间匹配对三肇凹陷扶杨油层油成藏的控制作用[J].吉林大学学报(地球科学版), 2009, 39(4):656~661. http://www.cqvip.com/QK/91950X/201005/35585261.html
WANG Yachun, WANG Shengnan. Controlling of the match of source rock, overpressure and fault on oil accumulation of Fu-Yang oil layer in sanzhao depression[J]. Journal of Jilin University (Earth Science Edition), 2009, 39(4):656~661. (in Chinese with English abstract) http://www.cqvip.com/QK/91950X/201005/35585261.html
Pironon J, Canals M, Dubessy J, et al. Volumetric reconstruction of individual oil inclusions by confocal scanning laser microscopy[J]. European Journal of Mineralogy, 1998, 10(6):1143~1150. doi: 10.1127/ejm/10/6/1143
李荣西, 金奎励, 廖永胜.有机包裹体显微傅里叶红外光谱和荧光光谱测定及其意义[J].地球化学, 1998, 27(3):244~250. http://kns.cnki.net/KCMS/detail/detail.aspx?filename=dqhx199803004&dbname=CJFD&dbcode=CJFQ
LI Rongxi, JIN Kuili, LIAO Yongsheng. Analysis of organic inclusions using micro-FT. IR and fluorescence microscopy and its significance[J]. Geochemica, 1998, 27(3):244~250. (in Chinese with English abstract) http://kns.cnki.net/KCMS/detail/detail.aspx?filename=dqhx199803004&dbname=CJFD&dbcode=CJFQ
李兆奇, 陈红汉, 刘惠民, 等.流体包裹体多参数综合划分东营凹陷沙三段油气充注期次及充注时期确定[J].地质科技情报, 2008, 27(4):69~74. http://doi.wanfangdata.com.cn/10.3969/j.issn.1000-7849.2008.04.012
LI Zhaoqi, CHEN Honghan, LIU Huimin, et al. Division of hydrocarbon charges and charging date determination of Sha 3 member, Dongying depression by various aspects of fluid inclusions[J]. Geological Science and Technology Information, 2008, 27(4):69~74. (in Chinese with English abstract) http://doi.wanfangdata.com.cn/10.3969/j.issn.1000-7849.2008.04.012
Munz I A. Petroleum inclusions in sedimentary basins:systematics, analytical methods and applications[J]. Lithos, 2001, 55(1/4):195~212. https://www.sciencedirect.com/science/article/pii/S0024493700000451