冀西北宣化盆地侏罗纪九龙山组凝灰岩形成时代、构造环境及地质意义

杨济远; 李杰; 白春东; 张家辉; 胡新茁; 田颖; 刘蓓蓓; 许凡; 齐朋超

doi:10.12401/j.nwg.2023162

冀西北宣化盆地侏罗纪九龙山组凝灰岩形成时代、构造环境及地质意义

1.
河北省区域地质调查院，河北省地学旅游研究中心，河北廊坊　065000

2.
中国地质调查局天津地质调查中心，天津　300170

3.
中国地质调查局前寒武纪地质研究中心，天津　300170

4.
中国地质调查局廊坊自然资源综合调查中心，河北廊坊　065000

5.
河北省地矿局第六地质大队，河北石家庄　050000

基金项目: 河北省自然资源厅项目“河北省沙岭子、宣化县、深井镇、涿鹿县1∶5万区域地质调查”（4540401JBND1G1）。

详细信息

作者简介: 杨济远（1990−），男，工程师，从事矿产地质与区域地质调查工作。E−mail：yangjiyuanda@163.com

通讯作者: 李杰（1985−），男，硕士，高级工程师，从事矿产地质与区域地质调查工作。E−mail：yinhelijie@163.com

中图分类号: P581

收稿日期: 2022-06-05

修回日期: 2023-07-23

刊出日期: 2023-12-20

Formation Age, Tectonic Setting and Geological Significance of The Jurassic Jiulongshan Formation Tuff in Xuanhua Basin, Northwest Hebei

1.
Hebei Institute of Regional Geological Survey, Geotourism Research Center of Hebei Province, Langfang 065000, Heibei, China

2.
Tianjin Center of China Geological Survey, Tianjin 300170, China

3.
Precambrian Geological Research Center, ChinaGeological Survey, Tianjin 300170, China

4.
Langfang Natural Resources Integrated Survey Center, China Geological Survey, Langfang 065000, Heibei, China

5.
The Sixth Geological Brigade of Hebei Bureau of Geology and Mineral Resources, Shijiazhuang 050000, Heibei, China

More Information

Corresponding author: LI Jie, yinhelijie@163.com

Received Date: 05 June 2022

Revised Date: 23 July 2023

Publish Date: 20 December 2023

摘要

摘要:
冀西北宣化盆地九龙山组陆相沉积地层发育，但地层的时代归属缺少化石和同位素测年资料佐证。研究区杨家营−响水铺一带九龙山组中下部发育流纹质凝灰岩夹层，为准确确定宣化盆地九龙山组的时代和形成环境，笔者对流纹质凝灰岩采集了锆石U−Pb同位素测年样品和岩石地球化学分析样品，获得了（161.9±0.8）Ma的²⁰⁶Pb/²³⁸U加权平均年龄值（LA−ICP−MS法），为晚侏罗世早期。岩石化学特征表明，流纹质凝灰岩属高Si、高K钙碱性过铝质岩石；稀土元素配分模式曲线为右倾型，轻稀土强烈富集，负Eu异常不明显；富集大离子亲石元素（Rb、K、Th、U），亏损Sr和高场强元素（Nb、Ti）。岩石地球化学特征显示其形成于挤压构造背景。锆石Hf同位素ε_Hf（t）值为−33.79～−2.71，二阶段亏损模式年龄（t_DM2）为1179～3323 Ma，表明流纹质凝灰岩岩浆多为古元古代—中元古代加厚的下地壳熔融形成。综合分析认为，宣化盆地九龙山组形成于中侏罗世晚期—晚侏罗世早期的挤压构造背景，该研究成果为研究九龙山组的时代归属、形成环境提供了新资料。
- 九龙山组 /
- LA−ICP−MS锆石U−Pb定年 /
- Hf同位素 /
- 宣化盆地
Abstract:
The continental sedimentary strata of the Jiulongshan Formation in the Xuanhua basin in Northwest Hebei are well developed, but the age of the strata is lacking in evidence from fossils and isotope dating data. In the Yangjiaying−Xiangshuipu area of the study area, rhyolitic tuff interlayers develop in the middle and lower parts of the Jiulongshan Formation. In order to accurately determine the age and formation environment of the Jiulongshan Formation in the Xuanhua Basin, the author collected zircon U−Pb isotope dating samples from the rhyolitic tuff and rock geochemical analysis samples. The ²⁰⁶Pb/²³⁸U weighted average age (LA−ICP−MS method) of (161.9±0.8) Ma was obtained, which is the early Late Jurassic. The petrochemical characteristics show that the rhyolitic tuff is a high−silicon, high−potassium calc−alkaline peraluminous rock; the distribution pattern curve of rare earth elements is right−dipping, with strong enrichment of light rare earths and no obvious negative Eu anomaly; the enrichment of large ions is lithophilic elements (Rb, K, Th, U), depleted Sr and high field strength elements (Nb, Ti). The geochemical characteristics of the rocks show that it was formed in a compressional tectonic setting. The zircon Hf isotope εHf(t) value is between −33.79～−2.71, and the second−stage depletion model age (t_DM2) is between 1179～3323 Ma, indicating that the rhyolitic tuff magma is mostly Paleoproterozoic−Mesoproterozoic thickened lower crust Melted to form. According to comprehensive analysis, the Jiulongshan Formation in Xuanhua basin was formed in the late Middle Jurassic−early Late Jurassic compressional structural setting. The research results provide new data for the study of the age attribution and formation environment of the Jiulongshan Formation.
- Jiulongshan formation /
- LA−ICP−MS zircon U−Pb dating /
- Hf isotope /
- Xuanhua basin

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图 1 冀西北宣化盆地一带地质简图（a据郑亚东等，2000修改；b据白春东等，2022修改）

Figure 1.

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图 2 宣化盆地杨家营–响水铺一带九龙山组实测剖面图（PM15）

Figure 2.

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图 3 宣化盆地杨营–响水铺一带九龙山组实测剖面图（PM42）

Figure 3.

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图 4 宣化盆地九龙山组流纹质凝灰岩野外露头和显微镜下图

Figure 4.

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图 5 宣化盆地九龙山组流纹质凝灰岩岩石学、岩石地球化学图

Figure 5.

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图 6 宣化盆地九龙山组流纹质凝灰岩原始地幔标准化微量元素蛛网图（a）和球粒陨石标准化稀土元素配分图（b）（标准值化值据Sun et al.，1989；b标准化值据Boynton et al.，1984）

Figure 6.

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图 7 宣化盆地九龙山组流纹质凝灰岩锆石锆石阴极发光图

Figure 7.

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图 8 宣化盆地九龙山组流纹质凝灰岩锆石U–Pb年龄谐和图

Figure 8.

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图 9 宣化盆地九龙山组流纹质凝灰岩锆石Hf同位素特征图（a据Yang et al.，2006；b据吴福元等，2007）

Figure 9.

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图 10 宣化盆地九龙山组底部砾岩与上部玄武岩接触宏观面貌图

Figure 10.

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图 11 宣化盆地九龙山组流纹质凝灰岩（Y+Nb）–Rb判别图解和Y–Nb判别图（据Pearce et al.，1984）

Figure 11.

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表 1 宣化盆地九龙山组流纹质凝灰岩主量元素（%）、微量元素（10⁻⁶）测试分析结果表

Table 1. Analysis results of major elements (%) and trace elements (10⁻⁶) of rhyolite tuff in Jiulongshan Formation in the Xuanhua Basin

样品号	PM15-15YQ2	PM15-16YQ2	PM15-23YQ2	PM42-7GP1	样品号	PM15-15YQ2	PM15-16YQ2	PM15-23YQ2	PM42-7GP1
SiO₂	72.59	73.43	73.57	72.81	In	0.03	0.03	0.03	0.03
TiO₂	0.25	0.29	0.24	0.15	W	0.90	1.01	0.70	0.65
Al₂O₃	13.28	13.25	13.49	13.91	Bi	0.13	0.13	0.13	0.21
Fe₂O₃	1.26	1.87	1.66	1.01	Cs	1.26	1.29	1.71	1.23
FeO	0.75	0.30	0.27	1.05	Ba	672.04	762.17	732.98	1166.14
MnO	0.08	0.08	0.05	0.07	La	31.74	35.65	34.34	49.38
MgO	0.87	0.82	0.58	0.23	Ce	60.14	68.20	64.50	85.29
CaO	1.58	0.97	0.68	0.55	Pr	6.57	7.53	7.00	8.09
Na₂O	4.34	4.10	3.48	4.79	Nd	22.27	25.82	22.94	27.74
K₂O	2.69	3.04	4.21	4.42	Sm	3.60	4.02	3.52	3.67
P₂O₅	0.07	0.09	0.06	0.04	Eu	0.83	0.98	0.80	1.14
灼失量	1.99	1.55	1.51	0.68	Gd	3.32	3.73	3.12	3.39
Total	99.84	99.83	99.85	99.83	Tb	0.48	0.48	0.43	0.42
A/NK	1.32	1.32	1.31	1.10	Dy	2.53	2.64	2.24	2.12
A/CNK	1.04	1.15	1.19	1.02	Ho	0.46	0.48	0.42	0.41
Li	21.48	25.58	17.01	17.42	Er	1.45	1.42	1.36	1.25
Be	1.48	1.61	1.97	1.91	Tm	0.24	0.24	0.24	0.22
Sc	5.83	6.11	7.60	2.60	Yb	1.35	1.36	1.38	1.42
V	27.04	29.43	25.94	18.54	Lu	0.28	0.26	0.27	0.23
Cr	10.11	13.12	7.24	5.15	Tl	0.36	0.41	0.56	0.93
Co	3.81	3.89	3.25	2.00	Pb	14.78	12.42	12.33	22.48
Ni	3.55	4.29	4.52	4.00	Th	6.52	6.49	7.18	11.59
Cu	6.54	7.86	7.11	8.51	U	1.46	1.47	1.97	2.40
Zn	43.23	49.33	42.18	34.56	Zr	116.03	128.87	125.81	138.01
Ga	14.87	14.66	15.79	13.35	Hf	2.98	3.03	2.86	4.27
Rb	71.20	77.36	107.06	117.92	∑REE	135.25	152.82	142.55	184.76
Sr	333.33	336.03	341.94	177.91	LREE	125.14	142.20	133.09	175.31
Y	116.03	128.87	125.81	138.01	HREE	10.10	10.62	9.46	9.45
Nb	16.99	17.02	15.85	11.80	LREE/HREE	12.39	13.39	14.07	18.54
Ta	15.73	16.19	18.47	13.58	La/Yb	16.85	18.77	17.80	25.01
Mo	0.88	0.81	0.94	1.16	δEu	0.73	0.77	0.74	0.98
Cd	0.40	0.55	0.62	0.51	δCe	1.02	1.02	1.02	1.05

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表 2 宣化盆地九龙山组流纹质凝灰岩LA–ICP–MS锆石U–Th–Pb定年测试结果表

Table 2. LA–ICP–MS zircon U–Th–Pb dating results of the rhyolite tuff in the Jiulongshan Formation in the Xuanhua basin

样号	Pb（10⁻⁶）	U（10⁻⁶）	Th（10⁻⁶）	Th/U	同位素比值						年龄（Ma）
					²⁰⁷Pb/²³⁵U		²⁰⁶Pb/²³⁸U		²⁰⁷Pb/²⁰⁶Pb		²⁰⁶Pb/²³⁸U		²⁰⁷Pb/²³⁵U		²⁰⁷Pb/²⁰⁶Pb
					比值	2σ	比值	2σ	比值	2σ	比值	2σ	比值	2σ	比值	2σ
1	15.9	428.0	510.0	0.84	0.1740	0.0100	0.0257	0.0007	0.0505	0.0027	163.4	4.2	162.6	8.6	200.0	120.0
2	8.3	172.5	260.7	0.66	0.1720	0.0110	0.0255	0.0004	0.0485	0.0032	162	2.7	160.2	9.6	110.0	140.0
3	8.6	126.8	280.0	0.45	0.1760	0.0130	0.0254	0.0005	0.0499	0.0037	162	3.1	164.0	11.0	130.0	150.0
4	5.5	117.6	177.0	0.66	0.1810	0.0110	0.0255	0.0005	0.0515	0.0030	162.3	3	169.5	9.7	220.0	120.0
5	10.0	167.9	336.2	0.50	0.1774	0.0082	0.0257	0.0004	0.0502	0.0024	163.4	2.2	165.1	7.0	162.0	100.0
6	3.4	77.7	107.8	0.72	0.1730	0.0140	0.0255	0.0005	0.0496	0.0041	162.5	3	161.0	12.0	80.0	160.0
7	14.7	269.5	483.6	0.56	0.1702	0.0072	0.0252	0.0003	0.0487	0.0022	160.3	2.1	159.2	6.3	109.0	93.0
8	13.7	337.0	455.4	0.74	0.1719	0.0088	0.0252	0.0005	0.0506	0.0027	160.8	2.7	160.7	7.6	190.0	110.0
9	16.4	282.5	558.0	0.51	0.1769	0.0076	0.0253	0.0005	0.0510	0.0021	161.1	3.2	164.8	6.5	210.0	89.0
10	16.8	319.7	542.7	0.59	0.1747	0.0060	0.0255	0.0003	0.0496	0.0018	162.5	2.1	163.1	5.2	153.0	74.0
11	13.2	329.6	452.7	0.73	0.1671	0.0090	0.0252	0.0005	0.0495	0.0028	160.6	3.2	156.6	7.9	150.0	120.0
12	9.2	155.9	305.9	0.51	0.1830	0.0160	0.0256	0.0006	0.0517	0.0045	163.1	3.4	170.0	13.0	230.0	180.0

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表 3 宣化盆地九龙山组流纹质凝灰岩锆石Hf同位素测试分析结果表

Table 3. Zircon Hf isotope analysis results of the rhyolitic tuff in the Jiulongshan Formation in the Xuanhua Basin

测点号	t（Ma）	¹⁷⁶Yb/¹⁷⁷Hf	¹⁷⁶Lu/¹⁷⁷Hf	¹⁷⁶Hf/¹⁷⁷Hf	2σ	εHf（t）	2σ	t_DM1（Ma）	t_DM2（Ma）	Lu/Hf
1	163.4	0.037086	0.001460	0.282453	0.907103	−7.84	0.91	1143	1703	−0.96
2	162.0	0.021016	0.000875	0.282506	0.871696	−5.94	0.87	1051	1582	−0.97
3	162.0	0.027908	0.001202	0.282496	0.903081	−6.32	0.90	1074	1606	−0.96
4	162.3	0.041201	0.001614	0.282494	0.988113	−6.45	0.99	1090	1614	−0.95
5	163.4	0.041546	0.001632	0.282529	0.768552	−5.20	0.77	1041	1536	−0.95
6	162.5	0.038554	0.001474	0.281720	0.962652	−33.79	0.96	2174	3323	−0.96
7	160.3	0.021689	0.000839	0.282494	0.914987	−6.40	0.92	1067	1610	−0.97
8	160.8	0.023269	0.000906	0.282437	0.952907	−8.40	0.95	1148	1736	−0.97
9	161.1	0.031761	0.001333	0.282532	0.848201	−5.11	0.85	1028	1529	−0.96
10	160.6	0.020550	0.000812	0.282465	0.770649	−7.41	0.77	1107	1674	−0.98
11	163.1	0.057856	0.002243	0.282601	1.036609	−2.71	1.04	953	1379	−0.93

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表 4 宣化盆地附近地区中晚侏罗世九龙山–髫髻山期同位素年龄数据表

Table 4. Middle and Late Jurassic Jiulongshan–Tiaojishan period isotopic age data in the area near the Xuanhua basin

序号	层位	采样地点	测试对象	年龄（Ma）	测试方法	资料来源
1	髫髻山组（下部）	北京十三陵	安山岩	161.1±1.9	Ar–Ar（plateau）	Davis et al.，2001
2	髫髻山组（底部）	北京十三陵	凝灰岩	157.2±1.2	U–Pb（LA–ICP–MS）	于海飞等，2016
3	髫髻山组（底部）	北京西山	粗安岩	156.6±3.1	U–Pb（SHRIMP）	赵越等，2004
4	髫髻山组（底部）	承德盆地	凝灰岩	160.7±0.8	Ar–Ar（plateau）	Davis et al.，2001
5	髫髻山组（底部）	承德盆地	凝灰岩	160.7±0.8	Ar–Ar（plateau）	Davis et al.，2001
6	髫髻山组（底部）	承德盆地	安山岩	159.7±1.3	Ar–Ar（plateau）	Cope，2003
7	九龙山组（下部）	承德盆地	凝灰岩	163.4±1.1	U–Pb（LA–ICP–MS）	陈海燕等，2014
8	九龙山组（下部）	宣化盆地	粗面岩	167.0	U–Pb（LA–ICP–MS）	王卫国等，2017
9	九龙山组（下部）	宣化盆地	凝灰岩	161.9±0.8	U–Pb（LA–ICP–MS）	本文

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冀西北宣化盆地侏罗纪九龙山组凝灰岩形成时代、构造环境及地质意义

作者简介: 杨济远（1990−），男，工程师，从事矿产地质与区域地质调查工作。E−mail：yangjiyuanda@163.com

通讯作者: 李杰（1985−），男，硕士，高级工程师，从事矿产地质与区域地质调查工作。E−mail：yinhelijie@163.com

Formation Age, Tectonic Setting and Geological Significance of The Jurassic Jiulongshan Formation Tuff in Xuanhua Basin, Northwest Hebei

Corresponding author: LI Jie, yinhelijie@163.com

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