中国地质学会岩矿测试技术专业委员会、国家地质实验测试中心主办

辽宁岫岩河磨玉岩石地球化学组成及锆石U-Pb定年研究

郑奋, 刘琰, 张红清. 辽宁岫岩河磨玉岩石地球化学组成及锆石U-Pb定年研究[J]. 岩矿测试, 2019, 38(4): 438-448. doi: 10.15898/j.cnki.11-2131/td.201807310089
引用本文: 郑奋, 刘琰, 张红清. 辽宁岫岩河磨玉岩石地球化学组成及锆石U-Pb定年研究[J]. 岩矿测试, 2019, 38(4): 438-448. doi: 10.15898/j.cnki.11-2131/td.201807310089
Fen ZHENG, Yan LIU, Hong-qing ZHANG. The Petrogeochemistry and Zircon U-Pb Age of Nephrite Placer Deposit in Xiuyan, Liaoning[J]. Rock and Mineral Analysis, 2019, 38(4): 438-448. doi: 10.15898/j.cnki.11-2131/td.201807310089
Citation: Fen ZHENG, Yan LIU, Hong-qing ZHANG. The Petrogeochemistry and Zircon U-Pb Age of Nephrite Placer Deposit in Xiuyan, Liaoning[J]. Rock and Mineral Analysis, 2019, 38(4): 438-448. doi: 10.15898/j.cnki.11-2131/td.201807310089

辽宁岫岩河磨玉岩石地球化学组成及锆石U-Pb定年研究

  • 基金项目:
    中国地质调查局"中国矿产地质志"二级项目(DD20160346, DD20190379);自然资源部中国地质调查局地质调查项目(DD20190060);国家自然科学基金项目(41772044)
详细信息
    作者简介: 郑奋, 研究生, 矿物学、岩石学、矿床学专业。E-mail:864902333@qq.com
    通讯作者: 刘琰, 副研究员, 矿物学、岩石学、矿床学专业, 主要从事稀土和稀有金属矿床研究。E-mail:ly@cags.ac.cn
  • 中图分类号: P597.3;O657.63

The Petrogeochemistry and Zircon U-Pb Age of Nephrite Placer Deposit in Xiuyan, Liaoning

More Information
  • 河磨玉是产于辽宁省岫岩县细玉沟沟谷及白沙河河谷底部和两岸阶地的和田玉,目前仅依据产出位置判断河磨玉来源于细玉沟沟头的原生和田玉矿床,但河磨玉的矿物组成、地球化学特征、年龄等并不清楚,与原生和田玉是否一致有待深入研究。本文主要通过电子探针成分分析、全岩主微量分析、氢氧同位素分析、锆石SHRIMP U-Pb定年等测试方法对河磨玉的矿物组成、地球化学特征及年龄进行研究,确定河磨玉与老玉是否为相同成因。结果表明:①河磨玉中主要矿物为透闪石、阳起石,次要矿物为透辉石、磷灰石、绿泥石、绿帘石、石英、榍石、锆石、磁铁矿、菱锌矿等。②河磨玉的成因类型为大理岩型。河磨玉稀土总量低,相对富集轻稀土,普遍显示Eu正异常。③河磨玉中透闪石δ18O值为8.00‰~10.60‰,δD值为-94.95‰~-75.20‰,成矿流体中的水主要为岩浆水。④河磨玉中的岩浆锆石U-Pb年龄为220.8±7.6Ma(n=4,MSWD=2.3),代表河磨玉成玉年龄的上限。本文提出河磨玉的稀土分配特征、氢氧同位素组成、成矿流体来源及形成年龄均与原生和田玉不一致,河磨玉并非来源于细玉沟沟头的原生和田玉。
  • 加载中
  • 图 1  河磨玉的显微照片及背散射电子图像

    Figure 1. 

    图 2  (a) 河磨玉与Jordanów和田玉全岩化学成分对比(改自Siqin等[10]), (b)河磨玉与Jordanów和田玉全岩Cr、Ni判别图(改自Adamo等[22])

    Figure 2. 

    图 3  河磨玉样品氢氧同位素特征

    Figure 3. 

    图 4  河磨玉的锆石阴极发光图像

    Figure 4. 

    图 5  河磨玉中锆石SHRIMP U-Pb年龄谐和图

    Figure 5. 

    表 1  河磨玉中透闪石-阳起石化学成分电子探针分析结果

    Table 1.  Chemical component analysis of tremolite and actinolite in Xiuyan placer nephrite obtained by EMPA

    样品编号 颜色 SiO2(%) TiO2(%) Al2O3(%) FeO(%) Cr2O3(%) MnO(%) MgO(%) CaO(%) Na2O(%) K2O(%) 总计(%) BFe2 BMg BCa CFe2 CMg Mg/(Mg+Fe2+) Mg/(Mg+Fe2+)平均比值 矿物定名
    LHM15-8-1 54.71 0.36 3.06 5.28 0.01 0.08 18.92 13.31 0.25 0.25 96.32 0.11 0.00 1.87 0.52 4.05 0.86
    LHM15-8-2 56.93 < 0.05 1.74 5.67 0.03 0.06 19.14 13.30 0.12 0.06 97.08 0.00 0.00 1.94 0.66 4.00 0.86
    LHM15-8-3 57.40 0.07 1.01 7.52 < 0.05 0.09 18.26 13.30 0.10 0.02 97.9 0.00 0.00 1.91 0.88 3.83 0.81
    LHM15-8-4 56.59 < 0.05 1.36 5.47 0.02 0.09 18.68 12.91 0.06 0.05 95.36 0.03 0.00 1.95 0.64 4.11 0.86
    LHM15-8-5 墨绿 56.28 0.03 1.83 5.57 < 0.05 0.15 18.92 13.30 0.13 0.05 96.38 0.06 0.00 1.91 0.60 4.07 0.86 0.87 阳起石
    LHM15-8-6 57.56 0.01 1.08 4.52 0.01 0.05 19.84 13.59 0.08 0.05 96.94 0.03 0.00 1.96 0.51 4.29 0.89
    LHM15-8-7 57.35 < 0.05 1.45 5.74 0.01 0.11 19.38 12.88 0.08 0.02 97.26 0.30 0.00 1.68 0.41 4.32 0.86
    LHM15-8-8 56.01 < 0.05 1.95 5.68 < 0.05 0.17 18.85 13.09 0.12 0.05 96.13 0.3 0.00 1.67 0.41 4.23 0.86
    LHM15-8-9 54.15 0.10 3.55 6.50 0.04 0.09 18.10 13.22 0.27 0.08 96.13 0.02 0.00 1.96 0.76 3.86 0.83
    LHM15-9-1 57.34 0.04 1.23 0.25 0.01 < 0.05 22.77 13.72 0.15 0.20 96.06 0.03 0.46 1.50 0.00 4.76 0.99
    LHM15-9-2 58.56 < 0.05 0.69 1.65 0.01 0.01 22.22 13.30 0.07 0.01 96.69 0.10 0.00 1.89 0.09 4.78 0.96
    LHM15-9-3 57.41 < 0.05 1.25 1.37 < 0.05 0.10 21.84 13.12 0.12 0.07 95.63 0.18 0.32 1.48 0.00 4.76 0.97
    LHM15-9-4 浅绿 57.83 < 0.05 0.31 1.00 < 0.05 0.07 22.39 13.62 < 0.05 0.03 95.47 0.12 0.05 1.80 0.00 4.94 0.98 0.96 透闪石
    LHM15-9-5 54.56 < 0.05 0.16 0.15 0.02 < 0.05 17.96 25.52 0.01 < 0.05 98.38 0.00 0.00 2.00 0.01 3.76 0.99
    LHM15-9-6 57.49 < 0.05 0.62 1.59 < 0.05 0.02 21.72 13.34 0.07 0.03 95.24 0.21 0.21 1.57 0.00 4.88 0.96
    LHM15-9-7 57.36 0.02 0.66 1.40 < 0.05 < 0.05 21.98 13.40 0.05 0.03 95.15 0.17 0.05 1.76 0.00 4.87 0.97
    LHM15-10-1 57.27 0.05 0.41 2.59 0.05 0.05 20.99 13.93 0.05 0.02 95.53 0.00 0.00 2.00 0.31 4.59 0.94
    LHM15-10-2 灰黑 56.80 < 0.05 0.44 3.41 0.01 0.07 21.10 13.88 0.01 0.01 95.83 0.01 0.00 1.97 0.39 4.52 0.92 0.94 透闪石
    LHM15-10-3 57.16 < 0.05 0.66 1.84 < 0.05 0.07 21.30 14.01 0.07 0.06 95.42 0.03 0.00 1.95 0.19 4.691 0.95
    LHM15-11-1 黄白 56.33 0.03 2.13 1.98 < 0.05 0.19 20.79 13.37 0.18 0.06 95.3 0.25 0.06 1.65 0.00 4.61 0.95 0.95 透闪石
    LHM15-11-2 57.99 0.10 0.34 1.94 0.01 0.28 21.63 13.38 0.02 0.02 95.92 0.06 0.00 1.89 0.17 4.75 0.95
    LHM15-11-3 58.34 0.03 0.75 1.69 < 0.05 0.22 22.00 13.30 0.07 0.01 96.44 0.00 0.00 1.83 0.19 4.52 0.96
    LHM15-11-4 57.14 0.11 1.13 2.12 0.01 0.14 21.68 12.81 0.08 0.06 95.43 0.18 0.00 1.79 0.07 4.72 0.95
    下载: 导出CSV

    表 2  河磨玉全岩主量元素分析结果

    Table 2.  Analytical results of major elements in Xiuyan placer nephrites

    主量元素 测定值(%)
    LHM15-1 LHM15-2 LHM15-3 LHM15-4 LHM15-5 LHM15-6 LHM15-7
    SiO2 59.37 57.95 58.72 58.96 58.92 59.50 59.39
    Al2O3 0.63 1.62 0.40 0.52 1.03 0.49 0.46
    CaO 12.72 11.94 12.63 11.97 12.28 12.59 12.87
    Fe2O3 < 0.05 < 0.05 0.49 0.11 0.05 < 0.05 < 0.05
    FeO 0.46 0.49 0.32 0.28 0.99 1.53 0.47
    K2O 0.10 0.09 0.05 0.06 0.06 0.05 0.06
    MgO 23.12 23.74 23.46 24.38 25.61 23.15 23.45
    MnO 0.05 0.06 0.06 0.06 0.05 0.06 0.05
    Na2O 0.10 0.05 0.07 0.13 0.10 0.05 0.05
    P2O5 0.04 0.03 0.07 0.12 0.07 0.07 0.03
    TiO2 0.02 0.01 < 0.05 < 0.05 0.01 < 0.05 0.01
    CO2 0.97 1.20 0.53 1.28 1.01 1.15 1.10
    H2O+ 1.66 1.98 1.86 2.04 1.54 1.18 1.12
    LOI 3.25 3.78 3.59 3.80 1.52 3.31 3.14
    下载: 导出CSV

    表 3  河磨玉全岩微量元素分析结果

    Table 3.  Analytical results of trace elements in Xiuyan placer nephrites

    微量元素 测定值(μg/g)
    LHM15-1 LHM15-2 LHM15-3 LHM15-4 LHM15-5 LHM15-6 LHM15-7
    Li 1.30 4.91 0.95 1.06 2.42 1.83 0.89
    Be 17.00 14.50 13.80 15.20 15.80 15.60 13.10
    Cr 6.26 2.93 0.91 2.32 1.72 1.68 12.20
    Mn 409 461 502 503 417 466 444
    Co 0.79 1.24 1.51 1.06 0.73 1.35 0.79
    Ni 1.08 0.81 < 0.05 1.11 0.86 0.74 6.19
    Cu 11.20 8.17 6.73 7.15 6.85 8.72 4.36
    Zn 30.10 56.70 53.80 44.10 37.90 29.40 41.30
    Ga 1.29 2.42 0.87 1.09 1.59 1.12 0.93
    Rb 1.82 1.22 0.56 1.34 1.01 1.00 0.93
    Sr 10.60 7.60 7.22 11.10 9.04 12.90 12.20
    Mo 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05
    Cd < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05
    In < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05
    Cs 0.52 0.39 0.26 0.56 0.33 0.49 0.32
    Ba 4.31 2.29 5.02 5.98 5.54 6.87 3.92
    Tl < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05
    Pb 1.75 0.49 0.64 1.45 4.09 1.35 0.39
    Bi < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05
    Th 0.45 0.10 < 0.05 0.05 < 0.05 < 0.05 < 0.05
    U 1.12 1.11 1.14 1.47 1.19 1.17 1.21
    Nb 0.56 0.53 0.67 0.49 0.47 0.49 0.38
    Ta 0.11 0.12 0.12 0.10 0.10 0.09 0.09
    Zr 5.31 0.77 1.12 0.83 0.95 0.48 0.50
    Hf 0.18 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05 < 0.05
    Sn 0.73 0.62 1.30 0.88 0.72 1.21 0.69
    Sb 5.09 5.18 1.52 4.72 2.78 2.86 2.12
    Ti 99.60 41.60 36.40 24.70 31.20 16.30 15.40
    W 0.26 0.17 0.48 0.34 0.19 0.25 0.25
    As 3.37 1.50 0.68 3.78 0.80 0.75 0.72
    V 11.40 15.80 8.25 11.20 9.56 10.10 9.17
    La 0.69 0.37 0.63 0.49 0.42 0.51 0.41
    Ce 1.59 0.81 1.56 1.09 1.03 1.08 0.96
    Pr 0.21 0.10 0.21 0.14 0.15 0.13 0.12
    Nd 1.04 0.48 1.12 0.70 0.82 0.67 0.64
    Sm 0.26 0.11 0.33 0.21 0.22 0.16 0.18
    Eu 0.08 0.07 0.14 0.12 0.07 0.08 0.08
    Gd 0.35 0.13 0.58 0.36 0.30 0.22 0.29
    Tb 0.08 < 0.05 0.15 0.10 0.07 0.06 0.08
    Dy 0.61 0.21 1.23 0.83 0.53 0.43 0.62
    Ho 0.14 0.05 0.30 0.21 0.12 0.10 0.15
    Er 0.38 0.15 0.93 0.63 0.32 0.31 0.41
    Tm 0.05 < 0.05 0.14 0.09 < 0.05 < 0.05 0.05
    Yb 0.29 0.12 0.90 0.55 0.22 0.25 0.29
    Lu < 0.05 < 0.05 0.16 0.08 < 0.05 < 0.05 < 0.05
    Sc 2.21 2.70 2.37 2.11 1.93 1.82 1.81
    Y 4.66 1.79 10.30 6.80 4.63 4.02 5.21
    下载: 导出CSV

    表 4  河磨玉的氢氧同位素数据

    Table 4.  Hydrogen and oxygen isotope data in Xiuyan placer nephrite

    样品编号 样品名称 δD(‰) δ18O(‰) δD(‰) δ18O(‰)
    330℃ 390℃ 450℃
    LHM15-1 透闪石 -88.23 8.40 -66.53 8.89 9.52 9.92
    LHM15-2 透闪石 -75.20 8.50 -53.50 8.99 9.62 10.02
    LHM15-3 透闪石 -93.29 8.80 -71.59 9.29 9.92 10.32
    LHM15-4 透闪石 -94.95 9.30 -73.25 9.79 10.42 10.82
    LHM15-5 透闪石 -78.51 10.60 -56.80 11.09 11.72 12.12
    LHM15-6 透闪石 -93.78 8.20 -72.07 8.69 9.32 9.72
    LHM15-7 透闪石 -86.58 8.00 -64.88 8.49 9.12 9.52
    下载: 导出CSV
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出版历程
收稿日期:  2018-07-31
修回日期:  2019-01-25
录用日期:  2019-04-09

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