Geochemical Characteristics and Geological Significance of Granites in Eastern Songliao Basin
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摘要:
笔者对松辽盆地东部与张广才岭西部含黑云母花岗岩进行LA–ICP–MS 测年和微量稀土元素地球化学分析，探究其成岩时代与成岩环境。样品锆石振荡生长环带明显，Th/U值较大，揭示其属于岩浆成因。锆石U–Pb测年测得年龄分别为（179.3±1.5） Ma和（177.5±1.4） Ma，属于早侏罗世末期。轻稀土元素分馏明显，重稀土元素无明显分馏，Eu、Ce元素具有正异常。样品形成于板块俯冲聚敛环境。该地区花岗岩在形成过程中主要受控于部分熔融作用，岩脉有地壳和地幔双重性，可能有地幔混染现象。通过统计大兴安岭、松辽盆地与张广才岭花岗岩年龄，发现张广才岭处花岗岩形成时期早于松辽盆地花岗岩形成时期，进一步验证前人推测古太平洋板块和蒙古–鄂霍茨克洋板块发生双俯冲+拆沉作用。
Abstract:LA–ICP–MS dating and trace REE geochemical analysis of biotite–bearing granites in the eastern part of Songliao basin and the western part of Zhangguangcai range are carried out to explore their diagenetic age and environment in this paper . The sample zircon oscillatory growth zone is obvious, and the Th/U ratio is big, indicating that it belongs to magmatic origin. The ages of zircon U–Pb dating are （179.3±1.5）Ma; （177.5±1.4）Ma, belonging to the end of Early Jurassic. Light rare earth elements have obvious fractionation, heavy rare earth elements have no obvious fractionation, and Eu and Ce elements have positive anomalies. The sample was formed in the subduction and accumulation environment of the plate. The formation of granites in the two regions is mainly controlled by partial melting. The two dikes have the duality of crust and mantle, may have mantle contamination. Based on the statistics of the ages of the granites in the Greater Khingan Mountains, Songliao basin and Zhangguangcai range, it is found that the granites in Zhangguangcai range were formed earlier than those in Songliao basin. Validate the previous speculation that the ancient Pacific plate and the Mongolia–Okhotsk ocean plate have double subduction and delamination.
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Key words:
- geochemistry /
- granite /
- U–Pb chronology /
- tectonic setting /
- Songliao basin
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图 9 Nb–Y构造环境判别图（据Pearce et al.，1984）
Figure 9.
表 1 绥化村花岗岩（S-SH-1）样品锆石测年结果表
Table 1. Zircon dating results of Suihuacun granite (S-SH-1) sample
点号 U Th Pb Th/U 同位素比值 年龄（Ma） 谐和度 （10–6） 207Pb/206Pb ± 1σ 207Pb/235U ± 1σ 206Pb/238U ± 1σ 207Pb/206Pb ± 1σ 207Pb/235U ± 1σ 206Pb/238U ± 1σ S-SH-1-001 787.25 424.80 26.99 0.54 0.0507 0.0017 0.1937 0.0066 0.0277 0.0006 229.0 76.4 179.8 5.6 176.1 3.9 98% S-SH-1-002 610.16 332.24 21.39 0.54 0.0496 0.0015 0.1940 0.0060 0.0283 0.0006 178.3 69.0 180.0 5.1 180.2 3.9 100% S-SH-1-003 580.54 263.11 20.33 0.45 0.0475 0.0014 0.1899 0.0057 0.0290 0.0006 73.2 69.3 176.5 4.9 184.3 4.0 96% S-SH-1-004 693.84 366.37 24.10 0.53 0.0509 0.0014 0.1980 0.0057 0.0282 0.0006 235.1 63.0 183.4 4.8 179.4 3.9 98% S-SH-1-006 565.66 289.23 19.66 0.51 0.0526 0.0015 0.2042 0.0061 0.0281 0.0006 312.7 64.6 188.7 5.1 178.9 3.9 95% S-SH-1-007 773.82 869.86 30.92 1.12 0.0499 0.0014 0.1938 0.0054 0.0282 0.0006 188.0 61.8 179.9 4.6 179.3 3.8 100% S-SH-1-008 622.87 324.97 21.32 0.52 0.0513 0.0016 0.1956 0.0060 0.0277 0.0006 252.5 67.9 181.4 5.1 176.0 3.8 97% S-SH-1-009 774.11 380.43 27.58 0.49 0.0477 0.0019 0.1928 0.0077 0.0293 0.0007 85.6 92.8 179.0 6.6 186.0 4.1 96% S-SH-1-010 853.63 384.03 28.68 0.45 0.0498 0.0013 0.1907 0.0051 0.0278 0.0006 187.2 58.7 177.2 4.3 176.4 3.8 100% S-SH-1-012 696.59 405.52 24.14 0.58 0.0518 0.0016 0.1969 0.0061 0.0276 0.0006 277.0 68.4 182.5 5.2 175.2 3.8 96% S-SH-1-013 778.72 385.45 27.03 0.49 0.0514 0.0014 0.2009 0.0055 0.0283 0.0006 259.1 60.3 185.9 4.7 180.2 3.9 97% S-SH-1-014 573.68 313.01 19.27 0.55 0.0496 0.0018 0.1851 0.0068 0.0271 0.0006 177.6 83.3 172.4 5.9 172.0 3.8 100% S-SH-1-015 689.19 347.64 23.77 0.50 0.0487 0.0014 0.1882 0.0055 0.0280 0.0006 132.3 65.9 175.1 4.7 178.2 3.8 98% S-SH-1-016 739.51 448.71 26.93 0.61 0.0497 0.0014 0.1975 0.0056 0.0288 0.0006 182.0 63.1 183.0 4.7 183.1 3.9 100% S-SH-1-017 755.55 375.12 25.37 0.50 0.0518 0.0018 0.1950 0.0068 0.0273 0.0006 276.4 76.7 180.9 5.7 173.6 3.8 96% S-SH-1-018 647.84 378.09 23.37 0.58 0.0503 0.0015 0.1979 0.0060 0.0286 0.0006 207.1 67.1 183.4 5.1 181.5 3.9 99% S-SH-1-021 358.56 151.36 12.04 0.42 0.0537 0.0022 0.2043 0.0082 0.0276 0.0006 358.8 88.3 188.7 6.9 175.4 3.9 93% S-SH-1-022 420.38 229.11 14.75 0.55 0.0513 0.0017 0.1987 0.0068 0.0281 0.0006 253.2 76.1 184.1 5.8 178.7 3.9 97% S-SH-1-023 665.75 352.93 23.82 0.53 0.0528 0.0015 0.2080 0.0060 0.0286 0.0006 321.1 63.2 191.8 5.1 181.5 3.9 94% S-SH-1-024 504.33 254.67 18.24 0.50 0.0506 0.0016 0.2041 0.0064 0.0293 0.0006 221.4 70.2 188.6 5.4 186.0 4.0 99% S-SH-1-026 760.81 399.46 26.73 0.53 0.0490 0.0014 0.1912 0.0055 0.0283 0.0006 148.1 64.3 177.7 4.7 179.9 3.9 99% S-SH-1-027 961.29 525.01 33.85 0.55 0.0514 0.0014 0.1983 0.0054 0.0280 0.0006 260.5 59.4 183.7 4.6 177.8 3.8 97% S-SH-1-028 821.54 599.28 30.68 0.73 0.0503 0.0014 0.1986 0.0056 0.0287 0.0006 206.5 62.3 184.0 4.7 182.2 3.9 99% S-SH-1-029 657.00 262.17 22.56 0.40 0.0517 0.0015 0.2025 0.0060 0.0284 0.0006 273.5 64.7 187.3 5.0 180.5 3.9 96% S-SH-1-030 675.37 361.07 24.49 0.53 0.0522 0.0016 0.2081 0.0065 0.0289 0.0006 293.8 68.7 192.0 5.5 183.8 4.0 96% 
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表 2 阿城区花岗岩（H-D-3）样品锆石测年结果表
Table 2. Zircon dating results of Acheng granite (H-D-3) samples
点号 U Th Pb Th/U 同位素比值 年龄（Ma） 谐和度 （10–6） 207Pb/206Pb ± 1σ 207Pb/235U ± 1σ 206Pb/238U ± 1σ 207Pb/206Pb ± 1σ 207Pb/235U ± 1σ 206Pb/238U ± 1σ H-D-3-001 646.04 389.25 23.40 0.60 0.0494 0.0014 0.1943 0.0058 0.0285 0.0006 166.4 66.9 180.3 4.9 181.3 3.9 99% H-D-3-002 1111.21 1061.47 42.11 0.96 0.0496 0.0012 0.1863 0.0048 0.0273 0.0006 175.3 57.4 173.5 4.1 173.3 3.7 100% H-D-3-003 928.60 557.41 33.19 0.60 0.0488 0.0013 0.1899 0.0051 0.0282 0.0006 139.0 59.9 176.6 4.3 179.4 3.8 98% H-D-3-004 362.17 310.08 13.71 0.86 0.0513 0.0017 0.1977 0.0067 0.0280 0.0006 253.3 75.5 183.2 5.7 177.8 3.9 97% H-D-3-005 550.99 343.51 19.96 0.62 0.0492 0.0015 0.1916 0.0060 0.0283 0.0006 156.1 70.0 178.0 5.1 179.7 3.9 99% H-D-3-006 1028.47 1121.34 41.04 1.09 0.0497 0.0013 0.1915 0.0050 0.0280 0.0006 180.1 57.8 177.9 4.3 177.7 3.8 100% H-D-3-007 356.46 203.77 12.61 0.57 0.0496 0.0017 0.1930 0.0067 0.0282 0.0006 174.6 78.8 179.2 5.7 179.5 3.9 100% H-D-3-008 274.01 207.36 10.25 0.76 0.0551 0.0020 0.2143 0.0080 0.0282 0.0006 415.1 80.2 197.1 6.7 179.4 3.9 91% H-D-3-009 239.30 232.46 9.27 0.97 0.0557 0.0021 0.2132 0.0082 0.0278 0.0006 439.1 83.6 196.3 6.9 176.6 3.9 89% H-D-3-010 891.02 865.63 33.06 0.97 0.0495 0.0013 0.1834 0.0050 0.0269 0.0006 169.2 60.5 171.0 4.3 171.1 3.7 100% H-D-3-011 1172.31 603.72 40.81 0.51 0.0497 0.0013 0.1924 0.0051 0.0281 0.0006 179.3 59.0 178.7 4.4 178.6 3.8 100% H-D-3-012 843.67 543.12 30.29 0.64 0.0490 0.0013 0.1887 0.0052 0.0279 0.0006 148.6 61.7 175.5 4.4 177.5 3.8 99% H-D-3-013 557.34 511.28 21.26 0.92 0.0486 0.0015 0.1872 0.0058 0.0279 0.0006 128.1 69.9 174.2 4.9 177.6 3.8 98% H-D-3-014 239.55 206.64 9.19 0.86 0.0494 0.0020 0.1928 0.0078 0.0283 0.0006 165.8 91.6 179.0 6.6 180.0 4.0 99% H-D-3-015 282.14 220.97 10.09 0.78 0.0506 0.0020 0.1874 0.0073 0.0269 0.0006 223.8 87.0 174.4 6.2 170.8 3.8 98% H-D-3-016 907.67 725.05 33.38 0.80 0.0493 0.0013 0.1876 0.0050 0.0276 0.0006 161.6 59.9 174.6 4.3 175.6 3.7 99% H-D-3-017 1217.89 1012.25 45.95 0.83 0.0494 0.0012 0.1911 0.0050 0.0280 0.0006 168.0 57.8 177.6 4.2 178.3 3.8 100% H-D-3-018 397.75 307.89 14.57 0.77 0.0498 0.0017 0.1893 0.0064 0.0276 0.0006 184.0 76.2 176.0 5.5 175.4 3.8 100% H-D-3-019 544.42 578.29 21.87 1.06 0.0488 0.0015 0.1903 0.0058 0.0283 0.0006 136.3 69.0 176.9 5.0 179.9 3.9 98% H-D-3-020 469.44 305.12 16.52 0.65 0.0505 0.0016 0.1904 0.0061 0.0273 0.0006 218.0 71.1 176.9 5.2 173.9 3.8 98% H-D-3-021 1057.08 420.85 35.81 0.40 0.0496 0.0013 0.1917 0.0051 0.0280 0.0006 175.2 59.7 178.0 4.4 178.3 3.8 100% H-D-3-022 1015.52 724.53 37.34 0.71 0.0483 0.0013 0.1858 0.0049 0.0279 0.0006 115.1 59.7 173.1 4.2 177.3 3.8 98% H-D-3-023 586.65 407.74 21.28 0.70 0.0488 0.0014 0.1876 0.0056 0.0279 0.0006 139.6 67.6 174.5 4.8 177.1 3.8 99% H-D-3-024 249.08 206.93 9.64 0.83 0.0472 0.0021 0.1858 0.0082 0.0286 0.0007 57.9 102.5 173.0 7.0 181.5 4.1 95% H-D-3-025 542.70 423.44 20.14 0.78 0.0506 0.0015 0.1946 0.0059 0.0279 0.0006 223.1 67.2 180.5 5.0 177.3 3.8 98% H-D-3-026 384.09 364.24 15.02 0.95 0.0513 0.0017 0.1998 0.0068 0.0282 0.0006 255.5 75.6 184.9 5.7 179.4 3.9 97% H-D-3-027 427.61 348.41 16.21 0.81 0.0518 0.0017 0.1992 0.0066 0.0279 0.0006 276.5 72.9 184.5 5.6 177.4 3.8 96% H-D-3-028 1109.09 648.61 39.08 0.58 0.0495 0.0013 0.1887 0.0049 0.0276 0.0006 171.6 58.0 175.5 4.2 175.8 3.7 100% H-D-3-029 130.61 73.88 4.72 0.57 0.0467 0.0030 0.1832 0.0115 0.0284 0.0007 35.4 144.9 170.8 9.9 180.7 4.2 94% H-D-3-030 707.68 276.05 24.24 0.39 0.0507 0.0014 0.1979 0.0057 0.0283 0.0006 227.7 63.8 183.3 4.8 179.9 3.9 98%
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表 3 绥化村花岗岩（S-SH-1）与阿城区花岗岩（H-D-3）花岗岩微量与稀土元素（10–6）
Table 3. Trace and rare earth elements of Suihuacun granite (S-SH-1) and Acheng granite (H-D-3) (10–6)
元素 SH1 SH2 SH3 SH4 SH5 SH平 H1 H2 H3 H4 H5 H平 Ti 2.52 3.23 2.78 5.15 1.75 3.09 9.94 5.85 2.95 5.52 9.92 6.84 Fe 10.17 13.58 41.84 17.72 17.56 20.17 3.65 4.12 2.12 2.69 2.29 2.97 Zr 4898.00 4898.00 4898.00 4898.00 4898.00 4898.00 4898.00 4898.00 4898.00 4898.00 4898.00 4898.00 Nb 4.31 4.52 4.19 4.28 4.85 4.43 1.16 4.29 5.89 1.00 2.49 2.97 Hf 139.88 146.23 142.79 143.53 147.32 143.95 109.15 129.19 142.22 116.40 118.78 123.15 Ta 1.91 1.94 1.70 1.99 2.24 1.96 0.44 1.37 1.93 0.35 0.90 1.00 Pb 21.39 24.10 19.66 21.32 26.93 22.68 9.27 33.06 30.29 9.64 16.21 19.70 Th 332.24 366.37 289.23 324.97 448.71 352.30 232.46 865.63 543.12 206.93 348.41 439.31 U 610.16 693.84 565.66 622.87 739.51 646.41 239.30 891.02 843.67 249.08 427.61 530.14 Y 9.41 9.64 9.00 9.64 10.37 9.61 10.68 18.00 19.43 10.97 13.58 14.53 La 13.87 11.96 27.79 9.55 17.39 16.11 5.80 11.12 15.82 2.32 2.18 7.45 Ce 77.35 59.24 95.88 58.60 82.09 74.63 28.43 58.08 66.51 27.36 30.62 42.20 Pr 4.07 3.28 9.02 2.94 5.11 4.88 1.78 3.37 2.28 0.81 0.73 1.79 Nd 15.58 14.37 34.55 13.17 20.03 19.54 9.74 17.12 8.04 6.11 5.23 9.25 Sm 4.75 4.75 7.83 4.70 6.33 5.67 6.18 9.71 5.53 5.82 5.82 6.61 Eu 0.41 0.34 0.55 0.48 0.61 0.48 1.67 1.82 1.07 1.53 1.46 1.51 Gd 0.16 0.16 0.17 0.15 0.18 0.16 0.26 0.40 0.32 0.28 0.28 0.31 Tb 0.05 0.05 0.05 0.05 0.06 0.05 0.08 0.13 0.12 0.08 0.09 0.10 Dy 0.71 0.73 0.69 0.72 0.78 0.73 0.94 1.52 1.52 0.95 1.13 1.21 Ho 0.28 0.30 0.28 0.29 0.32 0.29 0.35 0.56 0.60 0.35 0.43 0.46 Er 1.54 1.56 1.47 1.56 1.69 1.56 1.69 2.71 3.01 1.73 2.12 2.25 Tm 0.36 0.35 0.34 0.36 0.39 0.36 0.36 0.57 0.65 0.37 0.47 0.48 Yb 3.55 3.45 3.30 3.58 3.89 3.56 3.56 5.21 6.21 3.60 4.53 4.62 Lu 0.74 0.73 0.70 0.76 0.83 0.75 0.77 1.08 1.29 0.76 0.94 0.97 ∑REE 123.42 101.28 182.63 96.92 139.70 128.79 61.59 113.38 112.95 52.08 56.02 79.21 LREE 116.03 93.94 175.62 89.44 131.56 121.32 53.60 101.22 99.25 43.95 46.04 68.81 HREE 7.39 7.34 7.01 7.48 8.14 7.47 7.99 12.16 13.70 8.13 9.99 10.40 LREE/HREE 15.70 12.80 25.07 11.96 16.16 16.34 6.71 8.32 7.24 5.41 4.61 6.46 δEu 1.46 1.18 1.46 1.75 1.76 1.52 4.03 2.84 2.45 3.64 3.49 3.29 δCe 2.52 2.32 1.48 2.71 2.14 2.23 2.17 2.33 2.72 4.90 5.97 3.62 La/Yb 2.80 2.48 6.03 1.91 3.21 3.29 1.17 1.53 1.83 0.46 0.35 1.07 La/Sm 1.89 1.63 2.29 1.31 1.77 1.78 0.61 0.74 1.85 0.26 0.24 0.74 Gd/Yb 0.04 0.04 0.04 0.03 0.04 0.04 0.06 0.06 0.04 0.07 0.05 0.06
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