Study on Pore Structure and Quantitative Parameters of the Paleocene-Cretaceous Sandstone Reservoir in Jiangling Depression by SEM and Mercury Injection Method
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摘要: 通过储集层的孔喉结构来评价储层已广泛运用于油气开发,但目前尚未运用于钾盐储层的评价。本文利用扫描电镜和压汞法获得的大量储层孔隙、孔喉实验数据,研究了江汉盆地古新统—白垩系富钾卤水砂岩储层的孔喉类型和结构、毛细管压力曲线,以及孔喉定量特征参数。研究表明,古新统沙市组砂岩储层以Ⅱ类孔隙结构为主,排驱压力平均值为2.72 MPa,孔隙度平均值为6.32%。而白垩系红花套组砂岩储层以Ⅰ、Ⅱ类孔隙结构为主,Ⅰ类排驱压力平均值为0.28 MPa,孔隙度平均值为16.99%,渗透率为87.79×10-3 μm2;Ⅱ类排驱压力平均值为1.103 MPa,孔隙度平均值为10.02%,渗透率为18.83×10-3 μm2。通过综合分析孔喉定量特征参数(如最大汞饱和度、最大孔喉半径、中值半径、退汞效率等)来评价储层质量,认为古新统沙市组砂岩类型以粉砂岩为主,储层质量较差,属于特低孔低渗储层;白垩系红花套组砂岩类型以细砂岩为主,储层质量较好,属于低孔低渗储层。本研究为该区富钾卤水储层评价以及进一步勘探开发提供了可靠的地质依据。Abstract: Evaluating reservoirs by pore structure has been widely used in oil and gas development, but this method has not yet been used in the evaluation of potassium salt reservoirs. The pore throat type and structure, capillary pressure curve, and quantitative feature parameters of pore throat of the Paleocene-Cretaceous-rich potassium-rich brine reservoir in Jianghan basin are studied by using a large number of reservoir porosity and pore throat data obtained by Scanning Electron Microscopy and Mercury Intrusion. Combined with the discharge pressure and other experimental parameters, the pore structure is divided into Ⅰ, Ⅱ, and Ⅲ types. The results show that the sandstone reservoirs of the Paleocene Shashi Formation are dominated by type Ⅱ pore structure with the average displacement pressure of 2.72 MPa and the average porosity of 6.32%. The sandstone reservoirs of the Cretaceous Honghuatao Formation are dominated by Ⅰ and Ⅱ pore structure types. The displacement pressure of type Ⅰ is 0.28 MPa, the average porosity is 16.99%, and the permeability is 87.79×10-3 μm2. The average displacement pressure of type Ⅱ is 1.103 MPa, the average porosity is 10.02%, and the permeability is 18.83×10-3 μm2. The quality of the reservoir was evaluated by a comprehensive analysis of pore throat quantitative parameters such as maximum mercury saturation, maximum pore throat radius, median radius and mercury recovery efficiency. It is believed that the sandstone type of the Paleocene Shashi Formation is dominated by siltstone, and the quality of the reservoir is poor, which belongs to the low porosity and low permeability reservoir. The sandstone type of the Cretaceous Honghuatao Formation is mainly fine sandstone, and the reservoir is of good quality and belongs to low porosity and low permeability reservoir. This study provides a reliable geological basis for the evaluation of potassium-rich brine reservoirs and for further exploration and development.
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表 1 研究区砂岩储层孔喉定量特征参数统计
Table 1. quantitative characteristic parameters of pore throat of sandstone reservoir in study area
特征参数 古新统沙市组 白垩系红花套组 最小值 最大值 平均值 最小值 最大值 平均值 孔喉均值系数 0.6525 5.4958 2.7472 0.1779 2.8956 1.4707 孔喉分选系数 0.9733 2.4819 1.6331 0.9616 2.39 1.7739 孔喉歪度 0.1222 2.4463 1.5508 0.8373 2.6756 1.8246 变异系数 0.2043 2.6053 0.7919 0.5234 11.1296 1.65 中值压力 (MPa) 0.7981 53.5506 19.9596 0.924 70.5385 11.0217 中值半径 (μm) 0.0137 0.9563 0.1693 0.0104 0.8228 0.2013 排驱压力 (MPa) 0.408 27.2 8.8944 0.136 3.4 0.9568 最大吼道半径 (μm) 0.027 1.8025 0.3333 0.2163 5.4074 1.6841 最大汞饱和度 (%) 21.4415 95.9483 68.6512 29.3904 94.9398 70.045 退汞效率 (%) 6.8259 43.3264 27.3973 19.7878 54.6585 35.1276 平均孔喉比 1.3081 13.6501 3.2455 0.8295 4.0536 2.0408 -
[1] 肖佃师, 卢双舫, 陆正元, 等.联合核磁共振和恒速压汞方法测定致密砂岩孔喉结构[J].石油勘探与开发, 2016, 43(6):961-970. http://www.cnki.com.cn/Article/CJFDTOTAL-SKYK201606014.htm
Xiao D S, Lu S F, Lu Z Y, et al.Combining nuclear magnetic resonance and rate-controlled porosimetry to probe the pore-throat structure of tight sandstones[J].Petroleum Exploration and Development, 2016, 43(6):961-970. http://www.cnki.com.cn/Article/CJFDTOTAL-SKYK201606014.htm
[2] 操应长, 葸克来, 朱如凯, 等.松辽盆地南部泉四段扶余油层致密砂岩储层微观孔喉结构特征[J].中国石油大学学报 (自然科学版), 2015, 39(5):7-17. http://www.cnki.com.cn/Article/CJFDTOTAL-SYDX201505002.htm
Cao Y C, Xi K L, Zhu R K, et al.Microscopic porethroat characteristics of tight sandstone reservoirs in Fuyu Layer of the fourth member of Quantou Formation in Southern Songliao basin[J].Journal of China University of Petroleum (Natural Science), 2015, 39(5):7-17. http://www.cnki.com.cn/Article/CJFDTOTAL-SYDX201505002.htm
[3] Yao Y B, Liu D M.Comparison of low-field NMR and mercury intrusion porosimetry in characterizing pore size distribution of coals[J].Fuel, 2012, 95(1):152-158. http://www.sciencedirect.com/science/article/pii/S0016236111008088
[4] Clarkson C R, Jensen J L, Pedersen P K, et al.Innovative methods for flow-unit and pore-structure analysis in a tight siltstone and shale gas reservoir[J].AAPG Bulletin, 2012, 96(2):355-374. doi: 10.1306/05181110171
[5] 李爱芬, 任晓霞, 王桂娟, 等.核磁共振研究致密砂岩孔隙结构的方法及应用[J].中国石油大学学报 (自然科学版), 2015, 39(6):92-98. http://www.cnki.com.cn/Article/CJFDTOTAL-SYDX201506012.htm
Li A F, Ren X X, Wang G J, et al.Characterization of pore structure of low permeability reservoirs using a nuclear magnetic resonance method[J].Journal of China University of Petroleum (Natural Science), 2015, 39(6):92-98. http://www.cnki.com.cn/Article/CJFDTOTAL-SYDX201506012.htm
[6] 窦文超, 刘洛夫, 吴康军, 等.基于压汞实验研究低渗储层孔隙结构及其对渗透率的影响——以鄂尔多斯盆地西南部三叠系延长组长7储层为例[J].地质论评, 2016, 62(2):502-511. http://www.cnki.com.cn/Article/CJFDTOTAL-DZLP201602022.htm
Dou W C, Liu L F, Wu K J, et al.Pore structure characteristics and its effect on permeability by mercury injection measurement:An example from Triassic Chang-7 reservoir, Southwest Ordos basin[J].Geological Review, 2016, 62(2):502-511. http://www.cnki.com.cn/Article/CJFDTOTAL-DZLP201602022.htm
[7] Torabi A, Fossen H, Braathen A.Insight into petrophy-sical properties of deformed sandstone reservoirs[J].AAPG Bulletin, 2013, 97(4):619-637. doi: 10.1306/10031212040
[8] 杨峰, 宁正福, 孔德涛, 等.高压压汞法和氮气吸附法分析页岩孔隙结构[J].天然气地球科学, 2013, 24(3):450-455. http://www.cnki.com.cn/Article/CJFDTOTAL-TDKX201303002.htm
Yang F, Ning Z F, Kong D T, et al.Pore structure of shales from high pressure mercury injection and nitrogen adsorption method[J].Natural Gas Geoscience, 2013, 24(3):450-455. http://www.cnki.com.cn/Article/CJFDTOTAL-TDKX201303002.htm
[9] 陈生蓉, 帅琴, 高强, 等.基于扫描电镜-氮气吸脱附和压汞法的页岩孔隙结构研究[J].岩矿测试, 2015, 34(6):636-642. http://www.ykcs.ac.cn/ykcs/ch/reader/view_abstract.aspx?file_no=20150606&flag=1
Chen S R, Shuai Q, Gao Q, et al.Analysis of the pore structure of shale in Ordos Basin by SEM with nitrogen gas adsorption-desorption[J].Rock and Mineral Analysis, 2015, 34(6):636-642. http://www.ykcs.ac.cn/ykcs/ch/reader/view_abstract.aspx?file_no=20150606&flag=1
[10] 王羽, 金婵, 汪丽华, 等.应用氩离子抛光-扫描电镜方法研究四川九老洞组页岩微观孔隙特征[J].岩矿测试, 2015, 34(3):278-285. http://www.ykcs.ac.cn/ykcs/ch/reader/view_abstract.aspx?file_no=20150303&flag=1
Wang Y, Jin C, Wang L H, et al.Characterization of pore structures of Jiulaodong Formation shale in the Sichuan basin by SEM with Ar-ion milling[J].Rock and Mineral Analysis, 2015, 34(3):278-285. http://www.ykcs.ac.cn/ykcs/ch/reader/view_abstract.aspx?file_no=20150303&flag=1
[11] 刘亚伟, 张士万, 刘涛, 等.深层天然卤水特征及成因探讨——以江陵凹陷深层天然卤水研究为例[J].矿床地质, 2013, 32(6):1291-1299. http://www.cnki.com.cn/Article/CJFDTOTAL-KCDZ201306016.htm
Liu Y W, Zhang S W, Liu T, et al.Tentative discussion on features and genesis of deep natural brine:A case study of deep natural brine in Jiangling Depression[J].Mineral Deposits, 2013, 32(6):1291-1299. http://www.cnki.com.cn/Article/CJFDTOTAL-KCDZ201306016.htm
[12] 马黎春, 黄华, 张连元, 等.湖北潜江凹陷古近系深层富钾卤水矿床特征及成因[J].地质学报, 2015, 89(11):2114-2121. http://www.cnki.com.cn/Article/CJFDTOTAL-DZXE201511023.htm
Ma L C, Huang H, Zhang L Y, et al.Characteristics of paleogene deep potassium rich brines in the Qianjiang Depression, Hubei Province[J].Acta Geologica Sinica, 2015, 89(11):2114-2121. http://www.cnki.com.cn/Article/CJFDTOTAL-DZXE201511023.htm
[13] Lowenstein T K, Risacher F.Closed basin brine evolution and the influence of Ca-Cl inflow waters:Death valley and Bristol dry lake California, Qaidam basin, China, and Salar de Atacama, Chile[J].Aquatic Geochemistry, 2009(15):71-94. https://www.researchgate.net/publication/225590040_Closed_Basin_Brine_Evolution_and_the_Influence_of_Ca-Cl_Inflow_Waters_Death_Valley_and_Bristol_Dry_Lake_California_Qaidam_Basin_China_and_Salar_de_Atacama_Chile
[14] Nishio Y, Okamura K, Tanimizu M, et al.Lithium and strontium isotopic systematics of waters around Ontake volcano, Japan:Implications for deep-seated fluids and earthquake swarms[J].Earth & Planetary Science Letters, 2010, 297(3-4):567-576. https://www.researchgate.net/publication/222005841_Lithium_and_strontium_isotopic_systematics_of_waters_around_Ontake_volcano_Japan_Implications_for_deep-seated_fluids_and_earthquake_swarms
[15] 潘源敦, 刘成林, 徐海明.湖北江陵凹陷深层高温富钾卤水特征及其成因探讨[J].化工矿产地质, 2011, 33(2):65-72. http://www.cnki.com.cn/Article/CJFDTOTAL-HGKC201102002.htm
Pan Y D, Liu C L, Xu H M.Characteristics and genesis of deep high temperature potassium rich brine in Jiangling sag, Hubei[J].Geology of Chemical Minerals, 2011, 33(2):65-72. http://www.cnki.com.cn/Article/CJFDTOTAL-HGKC201102002.htm
[16] 易积正.江陵凹陷梅槐桥地区第三系新沟咀组下段沉积相及砂体分布研究[J].矿物岩石, 2010, 30(3):77-82. http://www.cnki.com.cn/Article/CJFDTOTAL-KWYS201003010.htm
Yi J Z.Research of sedimentary facies of lower Ex in Meihuaiqiao area, Jiangling Sag[J].Journal of Mineralogy and Petrology, 2010, 30(3):77-82. http://www.cnki.com.cn/Article/CJFDTOTAL-KWYS201003010.htm
[17] Roberto A, Sandstone V S.Carbonate petroleum reservoirs:A global perspective on porosity-depth and porosity-permeability relationships:Discussion[J].AAPG Bulletin, 2006, 90(5):807-810. doi: 10.1306/09140505131
[18] 邸世祥.中国碎屑岩储集层的孔隙结构[M].西安:西北大学出版社, 1991.
Di S X.Pore Structure of Clastic Reservoir in China[M].Xi'an:Northwestern University Press, 1991.
[19] 王国亭, 何东博, 李易隆, 等.吐哈盆地巴喀气田八道湾组致密砂岩储层分析及孔隙度演化定量模拟[J].地质学报, 2012, 86(11):1847-1856. doi: 10.3969/j.issn.0001-5717.2012.11.015
Wang G T, He D B, Li Y L, et al.Tight sandstone reservoir analysis and porosity-evolution quantitative simulation of the Badaowan Formation in the Baka gas field, Turpan-Hami basin[J].Acta Geologica Sinica, 2012, 86(11):1847-1856. doi: 10.3969/j.issn.0001-5717.2012.11.015
[20] 王培春, 李兴丽, 张琳琳, 等.利用常规测井物性曲线重构毛细管压力曲线[J].测井技术, 2012, 36 (1):33-36. http://www.cnki.com.cn/Article/CJFDTOTAL-CJJS201201010.htm
Wang P C, Li X L, Zhang L L, et al.The capillary pressure curve reconstruction based on conventional log physical properties[J].Well Logging Technology, 2012, 36(1):33-36. http://www.cnki.com.cn/Article/CJFDTOTAL-CJJS201201010.htm
[21] 赖锦, 王贵文, 柴毓, 等.致密砂岩储层孔隙结构成因机理分析及定量评价——以鄂尔多斯盆地姬塬地区长8油层组为例[J].地质学报, 2014, 88(11):2119-2130. http://www.cnki.com.cn/Article/CJFDTOTAL-DZXE201411009.htm
Lai J, Wang G W, Chai Y, et al.Mechanism analysis and quantitative assessment of pore structure for tight sandstone reservoirs:An example from Chang 8 oil layer in the Jiyuan area of Ordos basin[J].Acta Geologica Sinica, 2014, 88(11):2119-2130. http://www.cnki.com.cn/Article/CJFDTOTAL-DZXE201411009.htm
[22] 王国仓, 孙敏卓, 王鹏, 等.柴北缘马北8号构造下干柴沟组下段砂岩储层特征[J].石油学报, 2012, 33(2):242-248. http://www.cnki.com.cn/Article/CJFDTOTAL-SYXB201202009.htm
Wang G C, Sun M Z, Wang P, et al.Characteristics of the lower part of the Xiaganchaigou Formation in the Maber-Ⅷ structure in the Northern margin, Qaidam basin[J].Acta Petrolei Sinica, 2012, 33(2):242-248. http://www.cnki.com.cn/Article/CJFDTOTAL-SYXB201202009.htm
[23] 石媛媛, 洪才均, 房晓璐, 等.塔里木盆地库东—轮台地区苏维依组Ⅱ砂组沉积储层特征[J].石油实验地质, 2014, 36(4):422-427. doi: 10.11781/sysydz201404422
Shi Y Y, Hong C J, Fang X L, et al.Sedimentary reservoir characteristics of sandstone team Ⅱ of Suweiyi Formation in Kudong—Luntai area, Tarim basin[J].Petroleum Geology and Experiment, 2014, 36(4):422-427. doi: 10.11781/sysydz201404422
[24] 赵姗姗, 张哨楠, 万友利.塔中顺托果勒低隆区柯坪塔格组长石溶蚀及对储层的影响[J].石油实验地质, 2015, 37(3):293-299. doi: 10.11781/sysydz201503293
Zhao S S, Zhang S N, Wan Y L.Feldspar dissolution and its effect on reservoir in Kepingtage Formation, Shuntuoguole low uplift, Central Tarim basin[J].Petroleum Geology & Experiment, 2015, 37(3):293-299. doi: 10.11781/sysydz201503293
[25] 秦勇, 申建, 王宝文, 等.深部煤层气成藏效应及其耦合关系[J].石油学报, 2012, 33(1):48-54. doi: 10.7623/syxb201201006
Qin Y, Shen J, Wang B W, et al.Accumulation effects and coupling relationship of deep coalbed methane[J].Acta Petrolei Sinica, 2012, 33(1):48-54. doi: 10.7623/syxb201201006
[26] 成志刚, 罗少成, 杜支文, 等.基于储层孔喉特征参数计算致密砂岩渗透率的新方法[J].测井技术, 2014, 38(2):185-189. http://www.cnki.com.cn/Article/CJFDTOTAL-CJJS201402012.htm
Cheng Z G, Luo S C, Du Z W, et al.The method to calculate tight sandstone reservoir permeability using pore throat characteristic parameters[J].Well Logging Technology, 2014, 38(2):185-189. http://www.cnki.com.cn/Article/CJFDTOTAL-CJJS201402012.htm
[27] 徐丽, 王轶平, 段毅, 等.鄂尔多斯盆地南梁地区长4+5油层组储层特征[J].岩性油气藏, 2012, 24(4):34-39. http://www.cnki.com.cn/Article/CJFDTOTAL-YANX201204011.htm
Xu L, Wang Y P, Duan Y, et al.Reservoir characteristics of Chang 4+5 oil reservoir set in Nanliang area, Ordos basin[J].Lithologic Reservoirs, 2012, 24(4):34-39. http://www.cnki.com.cn/Article/CJFDTOTAL-YANX201204011.htm
[28] 李百强, 邱雅洁, 李洋, 等.鄂尔多斯盆地华庆地区长9储层微观孔隙结构特征[J].西安石油大学学报 (自然科学版), 2015, 30(5):10-15. http://www.cnki.com.cn/Article/CJFDTOTAL-XASY201505002.htm
Li B Q, Qiu Y J, Li Y, et al.Micro pore structure characteristics of Chang 9 reservoir in Huaqing area, Ordos basin[J].Journal of Xi'an Shiyou University (Natural Science), 2015, 30(5):10-15. http://www.cnki.com.cn/Article/CJFDTOTAL-XASY201505002.htm
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